Methods of Organic Compounds Identification A 1200-1MIZOAW6
Identification of compounds with chemical, spectroscopic and chromatographic methods
Topic of lectures.
1. Qualitative test for the elements.
2. Classification of compounds by solubility.
3.Tests for the functional grups.
a. Hydrocarbons;
b. Organohalogen compounds;
c. Alcohols;
d. Phenols;
e. Nitro compounds;
f. Amines and its salts;
Aldehydes and Ketones;
g. Arboxilic acids;
h. Derivatives of Carboxylic Acids.
4. Identification aminoacids and Carbohydrates.
5. Seperation of Mixtures of Organic Compounds.
6. Chromatography. Theory of Column Chromatography. Technique of Column Chromatography.
7. Aplication of Spectroscopic Methods for Structure Determination of organic Compounds.
a. Infrared Spectroskopy;
b. Hydrogen Nuclear Magnetic Resonanse Spectroscopy;
c. Carbon Nuclear Magnetic Resonanse Spectroskopy;
d. Ultraviolet-Visible Absorption Spectroscopy ( UV-VIS).
e. Mass Spectrometry (MS).
Type of course
Prerequisites (description)
Course coordinators
Mode
Learning outcomes
After the completion of the course the following tasks should be accomplished:
a) theoretical and applied know-how for structure determination of organic compounds,
b) general knowledge of chromatographic methods for separation and purification of organic compounds based on their physical state,
c) understanding how to determine the types of functional groups by spectroscopic methods,
d) ability to identify simply organic compounds by 1H-and 13C-NMR.
Assessment criteria
Exam test
Practical placement
Does not concern
Bibliography
1.J Mc Muray, Organic Chemistry, An International Thomson Publishing Company, 1996
2.R M. Silverstein , Francis X. Webster, David J. Kiemle, Spectrometric Identification of Organic Compounds, John Wiley and Sons Inc., 2005
Additional information
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