Analysis of Spectra 1200-2MON19Z
1. Analysis of 1D and 2D NMR spectra of the selected compounds with different structures, including substituted cyclohexanes and derivatives of bicyclo[3.2.1]octane.
2. Interpretation of spectra recorded using different NMR techniques.
3. 1H NOE spectra and their application for establishing the configuration of compounds.
4. Application of vicinal coupling constants in 1H NMR spectra for conformational analysis of compounds.
Estimated Student Workload (per semester): 32 hours
- attendance at lectures – 15 hours
- consultations – 2 hours
- preparation for the final examination – 15 hours
Main fields of studies for MISMaP
Course coordinators
Type of course
Mode
Learning outcomes
Upon completing the course students should be able to interpret 1D and 2D NMR spectra of organic compounds.
KNOWLEDGE: after passing the course, the student knows and understands:
K_W04- knows the aspects of the construction and operation of modern measuring equipment supporting scientific research in chemistry.
K_W05 - possesses in-depth knowledge and skills in the chosen chemical specialization, allowing the use of methods and concepts appropriate for this specialization and enabling independent research work.
SKILLS: After completing the course, the student is able to:
K_U03, - apply appropriate research methods, techniques, and tools within a given chemical specialization necessary to solve a defined
problem.
K¬U08 - demonstrate advanced knowledge and skills that allow for the effective use of professional literature, databases, and other information sources, as well as the ability to critically assess the reliability of obtained information.
SOCIAL COMPETENCES: After completing the course, the student is ready to:
K_K01 - engage in continuous learning and independently search for information in literature, including foreign languages.
Assessment criteria
The written examination will consist of independent interpretation of the 1H and 13C NMR spectra of the compound, which is mostly derived from cyclohexane or bicyclo[3.2.1]octane.
Practical placement
not applicable
Bibliography
1. Robert M. Silverstein, Francis X. Webster, David J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007.
2. Praca zbiorowa pod red. Mirosława Szafrana i Zofii Dega-Szafran, Określanie struktury związków organicznych metodami spektroskopowymi, PWN, 1988.