Crystallography Laboratory A 1200-2EN-CRALA1M
Experimental methods of X-ray crystallography: Laue method, oscillation method, goniometric methods; determination of unit cell parameters; Powder diffraction. Elements of crystallophysics. Interpretation of the crystal and molecular structure based on crystallographic databases
Estimated Student Workload (per semester): 50 hours
• Attendance at laboratories – 20 hours
• Consultations – 5 hours
• Preparation for each laboratory class – 10 hours
• Preparation for the final examination – 15 hours
Course coordinators
Type of course
Learning outcomes
Knowledge in presented topics
After completing the laboratory classes, the student:
Has knowledge and understanding of the fundamentals of crystallography, including the description of symmetry and crystal lattice structures, as well as X-ray crystallographic studies of crystals and the X-ray determination of the geometric structure of molecules.
Has knowledge of the basic aspects of the construction and operation of modern measurement apparatus supporting scientific research in the given chemical specialization.
Has a good understanding of current trends in the development of chemistry and the latest scientific discoveries in the given chemical specialization.
Is able to analyze the symmetry of selected molecules, polyhedral models of crystals, and crystal lattices.
Is able to apply X-ray methods to analyze the structure of crystals and molecules in the crystalline phase.
Possesses advanced knowledge and skills enabling the use of professional literature, databases, and other sources of information, as well as the ability to assess the reliability of obtained information.
Is able to present, in a way understandable also to non-specialists, the results of the most important discoveries made in the field of chemistry and related sciences.
Is able to independently acquire knowledge and develop professional skills using various sources (written and electronic), including foreign-language sources.
Has the ability to prepare oral presentations in Polish and English on topics related to selected chemical issues, using basic theoretical approaches and various sources.
Has a command of English sufficient to use basic professional literature in the field of chemistry and related sciences (at B2+ level).
Understands the need for and the possibilities of continuous professional development. Is able to independently search for information in the literature, including foreign-language sources.
Is able to work in a team and is aware of responsibility for jointly performed tasks related to teamwork.
Is convinced of the importance of professional conduct and adheres to the principles of professional ethics.
Is able to formulate opinions on professional issues and argue for them both among specialists and non-specialists.
Is able to think and act in a creative and entrepreneurial manner.
Assessment criteria
- activity 20-30%
- exam 70-80%
- obligatory participation in the laboratory
Practical placement
none
Bibliography
1. Z. Trzaska Durski, H. Trzaska Durska, Podstawy krystalografii strukturalnej i rentgenowskiej, Wydawnictwo Naukowe PWN, Warszawa, 1994 (in Polish).
2. Z. Bojarski, M. Gigla, K. Stróż, M. Surowiec, Krystalografia. Podręcznik wspomagany komputerowo, Wydawnictwo Naukowe PWN, Warszawa, 1996, 2001, 2007 (in Polish).
3. Z. Trzaska Durski, H. Trzaska Durska, Podstawy krystalografii, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa 2003 (in Polish).
4. P. Luger, Rentgenografia strukturalna monokryształów, PWN, Warszawa 1989 (in Polish).
5. M. van Meerssche i J. Feneau-Dupont, Krystalografia i chemia strukturalna, PWN, Warszawa 1984 (in Polish).
6. P. Luger, Modern X-ray Analysis on Single Crystals, Walter de Gruyter and Co., Berlin 1980 (in English).
7. C. Giacovazzo, H. Z. Monaco, D. Biterbo, F. Scordari, G. Gilli, G. Zanotti, M. Catti, Fundamentals of Crystallography, IUCR, Oxford University Press, 2000 (in English)