Advanced spectroscopy methods - laboratory 1200-2BLOK2-LAB1
The laboratory excersizes are intended to:
a) introduce practical aspects of application of spectroscopic methods in chemistry,
b) introduce student with mehodology of experiments and their interpretation.
Laboratory consists 10 excersizes inculding most important in chemistry spectroscopy techniques and their applications:
1. Analysis of functonal groups on the surface of grafene oxide,
2. Normal vibrations in molecules, how to determine them numerically, theory of groups, and femtosecond spectroscopy, wej.
3. Determination of H-Cl bond lenght from rotationastructure of IR sectra,
4. Silver nanoparticles featuring as surface in surface enhanced Raman scattering (SERS),
5. Investigation of fotodynamics of DCM colorant in polar and nonpolar solvents by femtosecond transient absorbtion,
6. Nuclear Overhauser effect,
7. Investigation of protein ligand interactions using NMR spectroscopy techniques,
8. Application of NMR spectroscopy for the implementation of quantum algorithms.
9. Investigation of oscilatory structure in I2 spctra on visible light and determination of disociation constant in excited state,
10. Application of resonance Raman effect for investigation of hemoglobin electronic strocture.
Each excersise last 6 hours.
Total student workload: 85 hours, consisting of:
1) Participation in classes: 60 hours
2) Preparation for classes: 10 hours
3) Preparation of reports: 15 hours
Main fields of studies for MISMaP
Type of course
Prerequisites (description)
Course coordinators
Learning outcomes
After passing the Laboratory student:
Has extensive knowledge of the place of chemistry in the system of exact and natural sciences and its importance for human development. - Knows and understands the theoretical foundations of various molecular spectroscopies. Knows the applications of various molecular spectroscopies. - Knows the basic aspects of the construction and operation of modern measurement equipment supporting scientific research in chemistry. - Has the mathematical knowledge necessary to quantitatively describe chemical phenomena and processes specific to a given chemical specialization. - Knows, understands, and can independently explain the mathematical description of basic chemical phenomena and processes. - Can use molecular spectroscopic methods to analyze the structure and properties of molecules in the gas and liquid phases.
Codes of acquired knowledge and competences.: K_W01, K_W04, K_W06, K_W07, K_W08,, K_W10, K_U03, K_U04, K_U05, K_U06, K_U07, K_U08, K_U09, K_U10, K_U11, K_U13, K_U15, K_U17, K_K01, K_K02, K_K03, K_K04, K_K05
Assessment criteria
At the beginning of each class, before performing the experimental work, students are required to pass an entrance test. The format of the test depends on the exercise.
After each exercise, students are required to complete a description and submit it no later than two weeks after completing the exercise. One joint description is required from each group.
Passing the exercise is contingent on:
a. passing the entrance test
b. active participation during the exercise
b. developing and submitting the description on time (including any exit test)
Passing the lab requires passing each exercise with a passing grade. The grade for the course is calculated as the average grade for all exercises.
Absences from classes require an excuse.
Delayed exercises can be completed in an additional lab. Only students who are missing no more than one exercise to pass the lab may participate in the additional lab.
At the beginning of each class, before completing the experimental work, students are required to pass an entrance test. The format of the test depends on the exercise.
After each exercise, students are required to complete a description and submit it no later than two weeks after completing the exercise. One shared description is required from each group.
Passing the exercise is contingent on:
a. the entrance test
b. active participation during the exercise
b. developing and submitting the description on time (including an exit test, if applicable)
Passing the exercise requires passing each exercise. The course grade is calculated as the average grade for all exercises.
Absences from classes require an excuse.
Delayed exercises can be completed in an additional workshop. Only students who are missing no more than one exercise to pass the workshop may participate in an additional workshop.
Bibliography
In Polish:
P. W. Atkins, Chemia Fizyczna, PWN, Warszawa, 2003.
Z. Kęcki, Podstawy spektroskopii molekularnej, PWN, Warszawa, 1992.
L. Stryer "Biochemia" PWN, Warszawa, 2003.
Biospektroskopia tomy 1-5 / pod red. Jacka Twardowskiego, Warszawa, PWN, 1989.
A. Ejchart, A. Gryff-Keller, „NMR w cieczach. Zarys teorii i metodologii”; Wydawnictwa Politechniki Warszawskiej, Warszawa 2003
In English:
a) Kensal E. van Holde, W. Curtis Johnson, P. Shing Ho Principles of physical biochemistry, Upper Saddle River, NJ, Pearson Education International, 2006. (Biblioteka Wydzialu Chemii UW)
b) Charles R Cantor, Paul R Schimmel Biophysical Chemistry Part I: The Conformation of Biological Macromolecules; Part II: Techniques for the Study of Biological Structure and Function; Part III: The Behavior of Biological Macromolecules, New York : W. H. Freeman and Company, 1980, 2001, 2002 (Biblioteka Wydzialu Chemii UW)
c) Donald T. Haynie Biological Thermodynamics Cambridge University Press, 2001.
d) SA Richards, JC Hollerton, Essential Practical NMR for organic chemistry, John Wiley and Sons, 2011
Additional information
Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system: