Automation in Chemical Analysis 1200-1ZMACHW6
The lecture covers the following topics:
*Development of mechanization and automation of analytical procedures over the years.
*Non-analytical automation (pre- and post-analytical). The concept of total laboratory automation.
*The role of mechanization and automation of analytical processes in modern chemical analysis (mainly in relation to clinical analysis, environmental protection, and food quality control).
*Presentation of the concepts and theoretical fundamentals of flow analyzers, discrete analyzers, centrifugal analyzers, as well as dry chemistry analyzers. Various designs of measuring equipment (including solutions for detection systems) and their applications in different areas of chemical analysis.
*The concept of miniaturization of analytical procedures, such as microfluidic systems, Lab-on-a-Chip, Lab-on-a-Foil, Lab-on-Paper/Paper-based Analytical Devices.
*Robotization of the analytical laboratory.
* Do-It-Yourself solutions versus mechanization/automation of analytical procedures.
Type of course
Course coordinators
Learning outcomes
After completing the lecture, the student:
*Analyzes possibilities for improving analytical procedures for the needs of routine applications in chemical analysis,
*Recognizes the possibilities of using various designs of mechanized instrumentation for analytical purposes,
*Designs measurement systems for flow analysis with various detection methods,
*Assesses the possibilities and limitations of applying different concepts for improving analytical measurements.
The student knows and understands:
K_W05 — At an advanced level, analytical chemistry in the scope of qualitative and quantitative analysis methods. Knows methods and techniques of instrumental analysis. Understands the relationship between signal and content. Knows and understands issues related to systematic and random errors. Knows methods for statistical interpretation of obtained results.
K_W14 — At an advanced level, aspects of design and operation of modern measuring equipment supporting scientific research in chemistry.
The student is able to:
K_U16 — Apply appropriate methods, techniques, and research tools within a given chemical specialty necessary to explain the posed problem, including advanced information and communication technologies.
K_U17 — Carry out measurements of selected physicochemical quantities, determine their values, and assess the reliability of the obtained results. Is able to operate selected measuring equipment.
K_U22 — Prepare written works in Polish and English on topics related to selected chemical issues using basic theoretical approaches as well as drawing on various sources.
The student is ready to:
K_K01 — Determine the scope of their own knowledge and skills and to improve professional and personal competences.
Assessment criteria
Exam covers the following topics:
*The concept of mechanization and automation of analytical processes (advantages and disadvantages, possibilities of their implementation, impact on analytical parameters).
*Pre- and post-analytical automation
*Discrete and centrifuge analyzers: basics of operation, design solutions, examples of applications, advantages and disadvantages of use.
*Theoretical principles of flow analysis: the concept of dispersion and its model description (dimensionless parameters, Ramsing equation, Taylor convection-diffusion equation).
*Types of flow techniques (basic elements of construction, detection methods).
*Possibility of processing samples in discrete and flow analyzers
*Main features of analyzers intended for clinical, food and environmental analysis.
Students participate in 30 hours of lectures, 15 hours of consultations, 20 hours of independent work based on materials provided by the instructor, and 15 hours of exam preparation. Two unexcused absences are permitted.
Practical placement
Professional training outside of the University is not needed for this course
Bibliography
1.M. Trojanowicz "Automatyzacja w analizie chemicznej" WNT, 1992.
2.B. Karlberg, G. E. Pacey "Wstrzykowa analiza przepływowa dla praktyków", WNT, 1994.
3. M. Trojanowicz "Advances in Flow Analysis", Wiley-VCH, 2008.
4. Materials and publications provided by the instructor.
Additional information
Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system: