Methods of Organic Compounds Identification B - seminar 1200-1MIZOBP6

The goal of the seminar is to gain ability to solve problems about separation of mixtures of organic compounds, determining their purity and identifying them.
Exercises solved during seminar refer to following subjects:
1. Chemical methods of compound identification
1.1 Chemical analysis of organic compound
- solubility groups
- functional group identification
1.2 Separating organic compound mixtures by classical methods
2. Chromatographic methods
- gas chromatography
- liquid (column) chromatography
- thin-layer chromatography
3. Spectroscopic methods
- ultraviolet-visible chromatography (UV-Vis)
- infrared chromatography (IR)
- nuclear magnetic resonance chromatography 1H NMR, 13C NMR
- mass spectrometry (MS)

Type of course

obligatory courses

Mode

Remote learning

Prerequisites (description)

Knowledge of basis of organic chemistry. The student should have a knowledge and should be able to apply various analytical and spectroscopic techniques. and techniques used in organic chemistry.

Course coordinators

Maciej Bagiński
Monika Góra
Wiktor Lewandowski

Learning outcomes

After the completion of the course the following tasks should be accomplished:
a) theoretical and applied know-how for structure determination of organic compounds,
b) general knowledge of chromatographic methods for separation and purification of organic compounds based on their physical state,
c) understanding how to determine the types of functional groups by spectroscopic methods,
d) ability to identify simply organic compounds by IR, 1H-, 13C-NMR and Mass Spectrometry (MS).

Assessment criteria

Mandatory attendance at all classes. Only 1 absence is allowed.
Absence during the final test must be excused with a sick leave.

Final test (open questions and problems to solve) - 100%

Active and prepared students will be rewarded with additional points that can positively affect the final grade.

Practical placement

not applicable

Bibliography

1. O. Demchuk, M. Topyła, K. Kapłon, „Ćwiczenia laboratoryjne z identyfikacji związków organicznych”, Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej, 2014.
2. K. Bańkowski, A. Krawczyk, R. Siciński, J. Stępiński, A. Temeriusz – Ćwiczenia z organicznej analizy jakościowej i chemii bioorganicznej - Wyd. UW, 1990.
3. A. Vogel - Preparatyka organiczna - WNT, 1984
4. R. Walczyna, J. Sokołowski, G. Kupryszewski - Analiza związków organicznych - Wyd. Uniw. Gdańskiego, 1996.
5. Z. Witkiewicz, Podstawy chromatografii i technik elektromigracyjnych, PWN, 2017
6. A. Berthillier - Chromatografia i jej zastosowanie - PWN, 1975.
7. Z. Witkiewicz – Podstawy chromatografii - WNT, 2000.
8. M. Szafran, Z. Dega-Szafran - Określanie struktury związków organicznych metodami spektroskopowymi - PWN, 1988.
9. R. M. Silverstein, F.X. Webster, D.J. Kiemle Spektroskopowe metody identyfikacji związków organicznych - PWN 2007.
10.F. Wehrli, T. Wirthlin - Interpretacja widm w spektroskopii 13C NMR - PWN, 1985
11. A. Ejchart, L. Kozerski - Spektroskopia magnetycznego rezonansu jądrowego 13C - PWN, 1981, 1988.
12. W. Zieliński, A. Rajca (red) - Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych - WNT, 1995.
13. C.N.R. Rao, – Spektroskopia elektronowa związków organicznych - PWNT, 1982.
14. B.D. Hames, N.M. Hooper, J.D. Houghton - Krótkie wykłady: Biochemia - PWN, 2001.
15. L. Kłyszejko-Stefanowicz - Ćwiczenia z biochemii - PWN, 1999.
16. R.K. Murray, D.K. Granner, P.A. Mayes, V.W. Rodwell - Biochemia Harpera - PZWL, 2004.
17. a) R.T. Morrison, R.N. Boyd - Chemia Organiczna - PWN, 1998. b) J. McMurry - Chemia Organiczna - PWN, 2005.

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 1200-1MIZOBP6 in USOSweb