Organic Chemistry Laboratory IIA 1200-1CHOR2AL4
During the classes, students work individually while following the health and safety regulations applicable in an organic chemistry laboratory.
At the beginning of the course, introductory exercises are carried out: purification of three organic substances through crystallization, simple distillation, and extraction. These exercises are preceded by demonstrations conducted by academic instructors.
After completing the introductory exercises, students must pass a test assessing their knowledge of basic purification techniques for organic compounds, the equipment used, types of drying agents, the ability to use chemical handbooks, simple calculations necessary for performing experiments correctly (e.g., converting concentrations, preparing solutions of a specific concentration, calculating reaction yields), and knowledge of safety regulations.
Next, the preparative part of the course is carried out, which involves synthesizing four compounds of increasing difficulty and time consumption. Before beginning the synthesis of each compound, students must pass an oral quiz with the instructor on the reaction mechanism, methods of obtaining the given class of compounds, their reactivity, and safety precautions.
At the end of the semester (students must complete at least three syntheses), a final written exam is held to assess theoretical and practical knowledge of organic synthesis.
Estimated student workload per semester – 150 hours, including:
Attendance in laboratory classes – 90 hours
Preparation for entry tests on syntheses – 20 hours
Preparation for technique quizzes and the final test – 20 hours
Preparation of laboratory reports – 20 hours
Main fields of studies for MISMaP
Type of course
Mode
Prerequisites (description)
Course coordinators
Term 2024L: | Term 2025L: |
Learning outcomes
KNOWLEDGE (K_W08, K_W15):
Upon completion of the course, the student:
Possesses advanced knowledge of organic chemistry and biochemistry (nomenclature, structure of organic compounds, chemical reactions, reaction mechanisms, synthesis methods, occurrence, and applications). Understands the significance of chemical phenomena in biological processes.
Has an advanced understanding of occupational health and safety principles sufficient for work in a chemical laboratory.
SKILLS (K_U08, K_U15, K_U17, K_U21, K_U28):
Upon completion of the course, the student:
Can analyze problems in the field of organic chemistry, including exploring mechanisms of organic reactions. Can carry out the synthesis of selected organic compounds. Can separate mixtures of organic compounds and purify the obtained substances.
Can skillfully plan and perform basic research and experiments in chemistry, observe and critically evaluate their results, and discuss sources of experimental error.
Can perform measurements of selected physicochemical quantities, determine their values, and assess the reliability of obtained results. Can operate selected measurement instruments.
Can independently acquire knowledge and develop professional skills using various sources (both written and electronic), including those in a foreign language.
Can plan and organize both individual and team work within joint projects and tasks, and critically evaluate the progress of such work.
SOCIAL COMPETENCIES (K_K01):
Upon completion of the course, the student is able to:
Recognize the scope of their knowledge and skills and is ready to improve their professional and personal competencies.
Assessment criteria
Attendance is mandatory. Two excused absences are allowed (however, all syntheses must be completed). Unexcused lateness exceeding 15 minutes is not permitted.
Course completion requirements:
Passing reports from the introductory exercises (distillation, crystallization, extraction).
Passing the entry test before each synthesis, followed by the individual performance and graded completion of the synthesis along with a written report.
Passing both the initial and final written quizzes. A minimum of 60% of the total points is required to pass.
Resit conditions:
Students who have not completed all practical exercises on time may complete one synthesis during the resit period. Failure to complete more than one synthesis prevents passing the course in the current semester.
Students who did not pass the final written quiz may retake it during the resit period.
For organisational matters, please contact Dr Katarzyna Sęktas.
Practical placement
Does not concern
Bibliography
Podstawy preparatyki organicznej, Skrypt dla studentów II roku Wydziału Chemii UW, Misicka A., Orłowska A., Piekarska-Bartoszewicz B., Witkowska E., LIBER, 2012 (wydanie II)
Preparatyka organiczna, Vogel A., WNT, 2006
Vogel's Textbook of Practical Organic Chemistry (5th Edition)
A.I. Vogel, A.R. Tatchell, B.S. Furnis, A.J. Hannaford, P.W.G. Smith
Additional information
Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system: